Al-intercalated acid activated bentonite beads for the …
It was reported that the polymeric composite beads prepared using alginate have specific characteristics such as high porosity, high surface area, high affinity in charged molecules, high ...
It was reported that the polymeric composite beads prepared using alginate have specific characteristics such as high porosity, high surface area, high affinity in charged molecules, high ...
The adsorption process requires adsorbent that is cheap and have high surface area. High surface area may results in increase in adsorption potential . A variety of materials have been used as adsorbent such as activated carbon, agricultural solid wastes, agricultural solid waste based on activated carbon, clay and minerals . …
bentonite showed good adsorptive properties and thermal stability. The analysis revealed that there is a rise in the specific surface area of the activated bentonite clay compared to that of the raw bentonite clay (from 41.7065 to 49.227 m²/g). Keywords-Acid-Activated, Bentonite, Modeling I. INTRODUCTION
DOI: 10.1016/J.FOODCHEM.2007.03.060 Corpus ID: 96018042; The effect of sulphuric acid activation on the crystallinity, surface area, porosity, surface acidity, and bleaching power of a bentonite
In contrast, activated clay (Fig. 3b) revealed a rugged and uneven surface of the adsorbent, providing a large surface area (1638.66 m 2 g −1) and porosity for adsorption. The adsorption capacity of the HCl-activated bentonite was almost three times higher than that of raw BCs.
It was confirmed that acid treatment is an economical (∼ $400/t) and effective way of preparing environmentally benign porous activated clay having high surface area, pore volume and ...
The Hançılı (Keskin, Ankara, Turkey) bentonite was activated with H2SO4 by dry method at 97 °C for 6 h to obtain optimum parameters for imparting a maximum bleaching power towards soybean oil.
Figure 2: SEM image at low and high resolution of a) Native and b) Activated bentonite 3.2 XRD Analysis The XRD results (data base of MDI Jade 6.3 version) revealed that the activated bentonite clay
Materials. In the study, RB and the required acid solutions were purchased from FUJIFILM Wako Pure Chemical Corporation (Japan). Acid-activated RB was prepared via the following method: Five grams of RB was mixed with 50 mL of sulfuric acid, nitric acid, and phosphoric acid solutions at concentrations of 1, 5, and 10 mol/L, respectively. The …
Characterization of the Synthesized SO 3 H-MWCNTs. The BET surface area of the synthesized SO 3 H-MWCNTs was measured at 230 m 2 /g, with the pore volume and diameter recorded at 0.76 cm 3 /g and 11 nm, respectively. This high BET surface area was because of inducing the repulsion force between SO 3 H and COOH …
The optimum procedure is recommended as follows: 5 mass% of sodium carbonate powder and 30 wt.% water are added to activate the bentonite ore for 24 h to prepare activated bentonite; 0.5 wt.% of ...
The number of and Bronsted acid sites was strongly increased by intercalating of aluminum polyhydroxyl into the acid treated samples. Pillaring also improved micropore volume and consequently specific surface area of the samples. Pillared acid-activated bentonite was used for alkylation of benzene with 1-decene in liquid phase conditions.
The author reported that an increase in acid concentration greatly increased the specific surface area of the activated bentonite clays from 63.4 m 2 g −1 to 202 m 2 g −1. They observed the maximum specific surface area of activated bentonite was obtained when the temperature and acid concentration increased simultaneously.
Semantic Scholar extracted view of "Preparation and characterization of acid-activated bentonite powders" by M. Önal et al. ... The Hançılı bentonite from Turkey shows significant changes in surface area, micro- and mesoporosity, surface acidity and acid strength with heating from 100 to 900°C for 2 h. The specific surface … Expand. 54. PDF.
Activated carbon (AC) has been widely used in food, medicine, air and water pollution control and other fields [1,2,3,4,5,6,7,8,9].Due to its good physical and chemical properties such as high mechanical strength, high specific surface area and chemical stability, AC becomes the most popular adsorption material, which can remove …
The evolution of surface properties, such as surface acid centres, porosity and specific surface area, in a bentonite from Almeria (Spain) after acid and heat treatments (0.25–2.00 N H2SO4 and 110–40°C) has been studied. The samples were characterized by mercury porosimetry and by X-ray diffraction. The number of surface …
This study aimed to investigate the characteristics of acid-activated bentonite by focusing on its capability of improving the quality of tap water used during wire electrical discharge machining. ... respectively. Scanning electron microscopy images, specific surface area, pore volume, cation exchange capacity, X-ray diffraction patterns, and ...
In this study, the adsorption of NH 3 gas on a bentonite from Ünye (Turkey) in its natural state and after acid treatments, was investigated experimentally at 298 K and up to 100 kPa. Bentonite was treated with HCl solutions of various concentrations (0.5–2.5 M) at …
The specific surface area of acid-activated bentonite was estimated using the methylene blue adsorption method. The morphology of untreated, activated, and HA-sorbed bentonite was studied under scanning electron microscope (SEM). ... [6,7], can be reasonably used in order to remove humic acid from water. Activated carbon exhibits a …
The BET surface area analysis revealed that acid-activated bentonite (AAB) possessed more than two fold higher surface area as compared to NB. Combining pH zpc measurements, effect of solution pH and CIP speciation revealed that CIP sorption onto bentonite is highly dependent on solution pH. Kinetic studies confirmed that CIP …
Natural bentonite was activated with 2 M sulfuric acid, 4.5 h and 95 °C (the best acid-activated sample with the highest adsorption capacity) and the other 6 M sulfuric acid, 7.5 h and 95 °C ...
Results were compared with commercial bentonite (Tonsil) having surface area (378 m2/g). The activated sample M1 during 4 h at 75 °C possesses a decolorizing capacity of about 85% greater than ...
Acid activation was carried out by heating muds prepared from Ca-rich bentonite (CaB), sulfuric acid (H 2 SO 4) and distilled water, yielding various bleaching earths (BEs).The roles of each of the process variables, namely mass fraction of H 2 SO 4 (x) in the dried CaB and pure H 2 SO 4 mixture, heating temperature (T) and contact time (t), in the …
DOI: 10.1016/J.APSUSC.2011.10.088 Corpus ID: 97754238; Simultaneous determination of cation exchange capacity and surface area of acid activated bentonite powders by methylene blue sorption
activated maximum. surface Key products area, were Bentonite, India acid carried and the were 45m2/g (raw to removal of Acid activation India bentonite are which one is of under Generally can be enhanced mainly alkaline for etc process products such acid area and of Decolorization adsorption pore and activated process smectites is process ...
The specific surface area and pore volume have an upward trend as the acid concentration increases, while they stabilize after 0.7 M (Figure 5). Table 2. Specific surface area and porosity of raw and treated AlBe-G bentonite (80 C; acid concentrations of 0.5 M, 0.7 M and 1 M; 2% of pulp density).
The adsorption of humic acid on bentonite from Milos Island (Greece) acid-treated with dilute H(2)SO(4) solutions over a concentration range between 0.25 and 13M has been studied.
The specific surface area and the textural properties of the acid-activated bentonite are strongly affected by the process parameters. The optimum conditions to obtain the maximum specific ...
The 5 M H 2 SO 4 treated bentonite clay having surface area (305 m 2 /g) and pore volume (0.113 cm 3 /g) when used as a catalyst in esterification reaction gave high conversion (62%) of succinic acid and high yield (73%) of diethyl succinate at moderate reaction conditions. This result clearly demonstrated that acid treatment is an …
The adsorption of humic acid on bentonite from Milos Island (Greece) acid-treated with dilute H(2)SO(4) solutions over a concentration range between 0.25 and 13M has been studied. Bentonite activated with 3M sulfuric acid (AAS) showed a higher efficiency in removing humic acid from aqueous solutions …